HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 15029957, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Hydroxy-6-methoxy-3,4-dihydronaphthalen-1(2H)-one | HCID 21862723 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 15029957 | HCID 15029957 | — |
Reaction Steps
Using a procedure analogous to Example 7 from 4.5 g (0.024 mole) of 5-hydroxy-6-methoxy-1-tetralone, 5.4 g (0.031 mole) of benzyl bromide and 10 g (0.072 mole of K2CO3 in 100 ml of acetone), the title product was obtained (5.13 g) as a white solid by crystallization with ether, mp. 90° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455572B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-e48ac64e28b54d11a6aa3f2c9e11b118 |
| Source note | uspto-grants-2002_09 |