HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 23469000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | N,N-dimethyl-1-(1H-pyrrol-2-yl)methanamine | HCID 260796 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 23469000 | HCID 23469000 | 52.1% |
Reaction Steps
A solution of 2-(dimethylaminomethyl)pyrrole (24.8 g) and imidazole (13.6 g) in xylene (120 ml) are heated under reflux for 3 hours. The solution was cooled and the solid was filtered off and crystallised from ether to give 2-(imidazol-1-ylmethyl) pyrrole (15.3 g), m.p. 89°-90°, raised to 91°-92° on further crystallisation from water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04259345 |
| Source dataset | uspto-grants-1981_03 |
| ORD ID | ord-a8d1fca8ea0a4ed1be314a99f5070d04 |
| Source note | uspto-grants-1981_03 |