HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1282393Generated: November 1, 2026
Chloropentafluorobenzene → HCID 178505971, compound
https://huagongshe.com/reaction/1282393
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Chloropentafluorobenzene | HCID 9579 | — |
| Reactant | HCID 178418365 | HCID 178418365 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178505971 | HCID 178505971 | — |
Reaction Steps
In a drybox, 31.45 g of chloropentafluorobenzene prepared as in Example 21 above (0.155 mole) and 64.42 g of a 2 molar ether solution of isopropylmagnesium bromide (iPrMgBr) (0.141 mole) are charged to a Fisher Porter reactor and heated to 60° C. for 4.5 hours. Pentafluorophenylmagnesium bromide is formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06455718B1 |
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| Source dataset | uspto-grants-2002_09 |
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| ORD ID | ord-7ac04129fedb4bda811564056a01a77e |
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| Source note | uspto-grants-2002_09 |
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