Methyl iodide → HCID 23468998, compound

Participants

Reaction Steps

A solution of methyl iodide (3.55 g) in dry ether (20 ml) was added dropwise to a stirred solution of 1-cyclohexyl-2-dimethylaminomethylpyrrole (4.12 g) in dry ether (50 ml) at 5°. The resulting mixture was stirred at room temperature for 5 hours and then allowed to stand overnight. The solid was filtered off, washed with ether and dried to give [1-cyclohexyl-pyrrol-2-yl]methyl trimethylammonium iodide (6.0 g), m.p.>250° (darkening ca. 190°).

Provenance & Evidence