HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzenesulfonyl chloride → Nepsilon-(4-nitrobenzenesulfonyl)-Nalpha-(9-fluorenylmethoxycarbonyl)-L-lysine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzenesulfonyl chloride | HCID 7404 | — |
| Reactant | (2S)-6-amino-2-({[(9H-fluoren-9-yl)methoxy]carbonyl}amino)hexanoic acid | HCID 7010557 | — |
| Product | Nepsilon-(4-nitrobenzenesulfonyl)-Nalpha-(9-fluorenylmethoxycarbonyl)-L-lysine | HCID 14258337 | 89% |
Reaction Steps
Nα-(9-fluorenylmethoxycarbonyl)-L-lysine was reacted with 4-nitrobenzenesulfonyl chloride under the conditions used in example 2 giving 89% of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455587B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-00ed482467af48cb8087238cd2798af7 |
| Source note | uspto-grants-2002_09 |