HRID1282484
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The product obtained from example 3 (553 mg, 1.00 mmol) was dissolved in EtOAc (10 mL) and then hydrogenated using 10% Pd on charcoal as catalyst at atmospheric pressure for 2 h. The catalyst was filtered off and the filtrate was evaporated in vacuo to yield the title compound in 95% yield.
WORKUP
后处理
- customfor 2 h
- filtrationThe catalyst was filtered off
- customthe filtrate was evaporated in vacuo