HRID1282502
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The product obtained from example 28 (54.0 mg, 0.10 mmol) was dissolved in MeOH (5 mL) and then hydrogenated using 10% Pd/C as catalyst at atmospheric pressure for 1 h. The catalyst was filtered off and the filtrate was evaporated in vacuo to yield 96% of the title compound.
WORKUP
后处理
- customfor 1 h
- filtrationThe catalyst was filtered off
- customthe filtrate was evaporated in vacuo