HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23385756, compound → HCID 23385753, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23385756 | HCID 23385756 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23385753 | HCID 23385753 | 96% |
Reaction Steps
The product obtained from example 28 (54.0 mg, 0.10 mmol) was dissolved in MeOH (5 mL) and then hydrogenated using 10% Pd/C as catalyst at atmospheric pressure for 1 h. The catalyst was filtered off and the filtrate was evaporated in vacuo to yield 96% of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455587B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-cf4cea4e534d4f69aa7d6eba5b46384d |
| Source note | uspto-grants-2002_09 |