HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethoxycinnamic acid → HCID 10122653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethoxycinnamic acid | HCID 99525 | — |
| Reactant | Nalpha-isobutyl-Nalpha-(4-methylbenzenesulfonyl)-L-lysine | HCID 23552860 | — |
| Product | HCID 10122653 | HCID 10122653 | 18% |
Reaction Steps
Nα-isobutyl-Nα-(4-methylbenzenesulfonyl)-L-lysine was reacted with 2,3-dimethoxycinnamic acid under the conditions described in example 86. The crude material was purified by flash chromatography (CH2Cl2:MeOH, 49:1 to 9:1) to yield 18% of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455587B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-07a7fc3721ae40749e925033d47f64d9 |
| Source note | uspto-grants-2002_09 |