HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenoxyacetyl chloride → HCID 513410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenoxyacetyl chloride | HCID 69703 | — |
| Reactant | Nalpha-isobutyl-Nalpha-(4-methylbenzenesulfonyl)-L-lysine | HCID 23552860 | — |
| Product | HCID 513410 | HCID 513410 | 77% |
Reaction Steps
Nα-isobutyl-Nα-(4-methylbenzenesulfonyl)-L-lysine was reacted with phenoxyacetyl chloride under the conditions described in example 2. The crude material was purified by flash chromatography (CH2Cl2:MeOH, 19:1 to 9:1) to yield 77% of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06455587B1 |
| Source dataset | uspto-grants-2002_09 |
| ORD ID | ord-969753b406a44e3b859cfb64cf5bf976 |
| Source note | uspto-grants-2002_09 |