HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 86732977, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | N-Carbamimidoyl-N-methylglycine--hydrogen chloride (1/1) | HCID 134732 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86732977 | HCID 86732977 | — |
Reaction Steps
Creatine hydrochloride (1.85 g., 0.01 mole) in methylene chloride (50 ml.) was treated with phosphorous pentachloride (2.06 g., 0.01 mole) at room temperature. The mixture was stirred overnight at room temperature and the acid chloride product filtered off, washed with methylene chloride and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972872 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-1fd4e25b6bdf4e658c06c86982933545 |
| Source note | uspto-grants-1976_08 |