HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → HCID 20158054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 21520171 | HCID 21520171 | — |
| Product | HCID 20158054 | HCID 20158054 | 30.4% |
Reaction Steps
2 g of 3-benzyl-4,6-dimethyl-2-pyrone, 6 g of 2-aminopyridine and 1 g of hydroxylamine-hydrochloride were heated for 8 hours to 70° C. After working up as described in Example 1, 0.65 g (30%) of 1-hydroxy-3-benzyl-4,6-dimethyl-2-pyridone were obtained; melting point 148° C (Calc.: 6.1 % N, found 6.1 % N).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972888 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-6c766eb7a64649babd9a8a242d6802df |
| Source note | uspto-grants-1976_08 |