Isopropanol → HCID 12771221, compound

HRID 1282746Notes

Reaction equation

HRID 1282746 reaction equation
Cl[C:2]([N:4]1[CH2:8][CH2:7][NH:6][C:5]1=[O:9])=[O:3].[CH:10]([OH:13])([CH3:12])[CH3:11]>O1CCOCC1>[CH:10]([O:13][C:2]([N:4]1[CH2:8][CH2:7][NH:6][C:5]1=[O:9])=[O:3])([CH3:12])[CH3:11]

Participants

4

Reactant 2

HCID 3776IsopropanolHCID 832412-Oxoimidazolidine-1-carbonyl chloride

Product 1

HCID 12771221HCID 12771221, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

14.9 parts by weight of N-chlorocarbonylimidazolid-2-one in 100 parts by volume of i-propanol and 100 parts by volume of dioxane were warmed to 50° C for 3 hours. After stripping off the solvent, the residue was recrystallized from acetone.

Workup

  1. customthe residue was recrystallized from acetone

Sources & evidence

ORD record
ord-dc3751d90fe2438eb3a8521b233fb7ed
Source dataset
uspto-grants-1976_08
Patent number
US03972870

Reaction notes

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