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HRID128283

反应详情

EQUATION

反应方程式

HRID 128283 的结构方程式

REACTANTS

反应物

2
结构：C[O-].[Na+]
HCID10942334

Methanol, sodium salt

CH3NaO

结构：CCOC(=O)CN(C)S(=O)(=O)c1c(C(=O)OC)sc2cc(C)ccc12
HCID23468714

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)C1=C(O)c2sc3cc(C)ccc3c2S(=O)(=O)N1C
HCID70578267

未命名化合物

收率 51%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Prepared analogous to Example 1(e) from methyl 3-{[(ethoxy-carbonyl-methyl)methylamino]sulfonyl}-6-methyl-benzo[b]thiophene-2-carboxylate by reaction with sodium methylate in anhydrous methanol with a yield of 51% of theory.