HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → N-(Trifluoroacetyl)-L-valyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 349-00-8 | HCID 2755241 | — |
| Product | N-(Trifluoroacetyl)-L-valyl chloride | HCID 54035397 | — |
Reaction Steps
A solution of 1 g. of N-trifluoroacetyl-L-valine in 5 ml. of thionyl chloride was cooled to 5°C. and stirred for 15 minutes. The excess thionyl chloride was removed under reduced pressure under a stream of dry nitrogen gas, affording N-trifluoroacetyl-L-valyl chloride as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972925 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-420b3c353f034e65996b1f623409410b |
| Source note | uspto-grants-1976_08 |