HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrobenzyl chloride → 2-Benzyl-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrobenzyl chloride | HCID 11921 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 2-Benzyl-nitrobenzene | HCID 315593 | — |
Reaction Steps
The reactions of this example use the procedures of Example 1. 2-Nitrobenzyl chloride is reacted with benzene to give 2-nitrodiphenylmethane which is reduced to 2-aminodiphenylmethane. The 2-aminodiphenylmethane is reacted with trifluoromethanesulfonic anhydride to give 2-benzyltrifluoromethanesulfonanilide, m.p. 55°-56.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03972926 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-fc2ce43dc9bf49dbb4eb393bfe5725b1 |
| Source note | uspto-grants-1976_08 |