2-Ethylhexylamine → HCID 21520378, compound

HRID 1282881Notes

Reaction equation

[CH2:1]([CH:3]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:4][NH2:5])[CH3:2].[C:10]([C:14]1[CH:15]=[C:16]([CH:20]=[C:21]([C:24]([CH3:27])([CH3:26])[CH3:25])[C:22]=1[OH:23])[C:17](O)=[O:18])([CH3:13])([CH3:12])[CH3:11]>>[CH2:1]([CH:3]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:4][NH:5][C:17](=[O:18])[C:16]1[CH:20]=[C:21]([C:24]([CH3:25])([CH3:26])[CH3:27])[C:22]([OH:23])=[C:14]([C:10]([CH3:13])([CH3:12])[CH3:11])[CH:15]=1)[CH3:2]

Participants

Reactant 2

HCID 77192-Ethylhexylamine

HCID 150073,5-Di-tert-butyl-4-hydroxybenzoic acid

Product 1

HCID 21520378HCID 21520378, compound

Procedure

In the manner of Example 7, 2-ethylhexylamine was reacted with 3,5-di-t-butyl-4-hydroxybenzoic acid to produce N-(2-ethylhexyl)-3,5-di-t-butyl-4-hydroxybenzamide; melting point 136°-140°C. When tested by the procedure of Example 2, this compound lasted 1000 hours, about 3.3 times as long as the control.

Sources & evidence

ORD record: ord-fc147f40c7cf4119a033cb9dea8f352e
Source dataset: uspto-grants-1976_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03972927

Reaction notes

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