HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diclofenac → HCID 21520578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diclofenac | HCID 3033 | — |
| Reactant | 2-(2-Hydroxyethyl)pyridine | HCID 7675 | — |
| Reactant | 1,1-Bis(2,2-dimethylpropoxy)-N,N-dimethylmethanamine | HCID 78623 | — |
| Product | HCID 21520578 | HCID 21520578 | — |
Reaction Steps
In analogous manner [o-(2,6-dichloro-anilino)-phenyl]-acetic acid-2-(2-pyridyl)-ethyl ester with a melting point of 67°-68°C (crystallisation from petroleum ether) is obtained starting from 2.96 g of [o-(2,6-dichloro-anilino)-phenyl]-acetic acid, 3.0 g of dimethyl formamide-dineopentylacetal, and 1.4 g of 2-(2-hydroxyethyl)-pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03973024 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-9525f945ad5248f68ce6bd677aaf3826 |
| Source note | uspto-grants-1976_08 |