Thionyl Chloride → HCID 12366428, compound

HRID 1282938Notes

Reaction equation

HRID 1282938 reaction equation
[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](O)=[O:7])=[C:4]([O:11][C:12](=[O:14])[CH3:13])[CH:3]=1.S(Cl)([Cl:17])=O>>[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([Cl:17])=[O:7])=[C:4]([O:11][C:12](=[O:14])[CH3:13])[CH:3]=1

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 1527825814504-07-5

Product 1

HCID 12366428HCID 12366428, compound

Procedure

4-Methyl-2-acetoxy-benzoic acid (18 g.) was dissolved in thionyl chloride (200 ml.), and the solution was left to stand overnight at room temperature. Removal of excess thionyl chloride by suction gave a paste of crude 4-methyl-2-acetoxy-benzoyl chloride which was dissolved in acetone (200 ml.).

Workup

  1. waitthe solution was left
  2. customRemoval of excess thionyl chloride by suction

Sources & evidence

ORD record
ord-7478949efd3346a183358223de32e16e
Source dataset
uspto-grants-1976_08
Patent number
US03973038

Reaction notes

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