HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 12366428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-Acetyl-4-methylsalicylicacid | HCID 15278258 | — |
| Product | HCID 12366428 | HCID 12366428 | — |
Reaction Steps
4-Methyl-2-acetoxy-benzoic acid (18 g.) was dissolved in thionyl chloride (200 ml.), and the solution was left to stand overnight at room temperature. Removal of excess thionyl chloride by suction gave a paste of crude 4-methyl-2-acetoxy-benzoyl chloride which was dissolved in acetone (200 ml.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03973038 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-7478949efd3346a183358223de32e16e |
| Source note | uspto-grants-1976_08 |