HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 21520539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 6-methyl-2-(thiophen-2-yl)quinoline | HCID 251366 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 21520539 | HCID 21520539 | — |
Reaction Steps
11.9 g of 2-(2-thienyl)-6-methyl-quinoline together with 360 ml of carbon tetrachloride, 10.4 g of N-bromosuccinimide and 0.3 g of dibenzoyl peroxide are boiled for 15 hours under reflux. The reaction mixture is cooled and filtered off. Concentration of the filtrate yields 2-(2-thienyl)-6-bromomethyl-quinoline which melts at 95°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03973022 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-70699420fc324ddb938ad37248bc0f76 |
| Source note | uspto-grants-1976_08 |