HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl vinyl ether → HCID 18512473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl vinyl ether | HCID 8023 | — |
| Reactant | Triethoxysilane | HCID 13830 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 18512473 | HCID 18512473 | 91% |
Reaction Steps
390 g vinylethylether, 600 g triethoxysilane, 3 g of a catalyst prepared according to Example 1 and 1000 ml of benzene were introduced into a reaction vessel and the mixture heated for 1.5 hours to boiling. After distillation, 786 g of CH3CH2OCH2CH2Si(OC2H5)3 were obtained (90% of the theoretical amount).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974095 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-677100ddcf1f474bbff1eaaa1b6fae90 |
| Source note | uspto-grants-1976_08 |