Ethyl vinyl ether → HCID 18512473, compound

HRID 1282982Notes

Reaction equation

HRID 1282982 reaction equation
[CH:1]([O:3][CH2:4][CH3:5])=[CH2:2].[CH2:6]([O:8][SiH:9]([O:13][CH2:14][CH3:15])[O:10][CH2:11][CH3:12])[CH3:7]>C1C=CC=CC=1>[CH3:2][CH2:1][O:3][CH2:4][CH2:5][Si:9]([O:13][CH2:14][CH3:15])([O:10][CH2:11][CH3:12])[O:8][CH2:6][CH3:7]

Participants

4

Reactant 2

HCID 8023Ethyl vinyl etherHCID 13830Triethoxysilane

Product 1

HCID 18512473HCID 18512473, compoundYield 91%

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

390 g vinylethylether, 600 g triethoxysilane, 3 g of a catalyst prepared according to Example 1 and 1000 ml of benzene were introduced into a reaction vessel and the mixture heated for 1.5 hours to boiling. After distillation, 786 g of CH3CH2OCH2CH2Si(OC2H5)3 were obtained (90% of the theoretical amount).

Workup

  1. additionwere introduced into a reaction vessel
  2. temperaturethe mixture heated for 1.5 hours
  3. distillationAfter distillation

Sources & evidence

ORD record
ord-677100ddcf1f474bbff1eaaa1b6fae90
Source dataset
uspto-grants-1976_08
Patent number
US03974095

Reaction notes

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