HRID1283070

反应详情

EQUATION

反应方程式

HRID 1283070 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Proceeding in a manner similar to that described in Example 1 above, 2-(p-tolyl)benzofuran (2.08 g; 0.01 mole) was interacted with 2.25 g (0.01 mole) of the anil derivative of terephthalaldehydic acid in the presence of 6.72 g (0.06 mole) of potassium tert-butoxide in 150 ml of dimethylformamide. The resulting product was purified by sublimation to obtain 2-[4-(4-carboxystyryl)phenyl]benzofuran which melted at 348°-349°C. The wavelength of maximum excitation of this compound was 365 nm and the wavelength of maximum emission was 425 nm.

WORKUP

后处理

  1. customThe resulting product was purified by sublimation