Ethyl Thioglycolate → HCID 21519310, compound

Participants

Reaction Steps

A stirred mixture of 3.25 g. of 4,6-dichloro-2-(p-chlorobenzylamino)pyrimidine, 1.35 g. of ethyl mercaptoacetate and 0.95 g. of sodium bicarbonate in 50 ml. of ethanol was heated under reflux overnight. The reaction mixture was filtered. A crystalline material was deposited which amounted to 2.7 g., m.p. 122°-125°C. The analytical sample was obtained by recrystallization from ethanol, m.p. 122°-125°C.

Provenance & Evidence