HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Glycolate → HCID 54447241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Glycolate | HCID 12184 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 21519299 | HCID 21519299 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54447241 | HCID 54447241 | — |
Reaction Steps
To 4.2 g. of ethyl glycolate in 50 ml. of anhydrous tetrahydrofuran was added 1.7 g. of sodium hydride oil dispersion (57 percent) with stirring. There was added after 20 minutes 11.5 g. of 2,4-dichloro-6-(p-chlorobenzylamino)pyrimidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974162 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-37d0c351035f462395e7775d0c3e1d96 |
| Source note | uspto-grants-1976_08 |