HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21519274, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 21519258 | HCID 21519258 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21519274 | HCID 21519274 | — |
Reaction Steps
A solution of 3.5 grams of 1-(2-dimethylamino-1-methylethyl)-2-phenyl-cyclohexanol in 250 ml ether and 10 ml tetrahydrofuran is treated with 6 ml methyl iodide and allowed to stand for 7 days. The crystalline product is filtered and washed with ether and recrystallized from water giving 2.1 grams melting at 155°-159°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974157 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-d523010a4cd2450b9bdfb6ac860fadda |
| Source note | uspto-grants-1976_08 |