HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 21519225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Cyclamate | HCID 7533 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 21519244 | HCID 21519244 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21519225 | HCID 21519225 | — |
Reaction Steps
The procedure of Example I (c) is followed using 7.5 g of 1-(2-Dimethylaminoethyl)-2-phenylcyclohexanol (Example XIV) and 8 ml of acetyl chloride with 18 ml triethylamine giving 11.8 g crude acetate which is treated with 12 g cyclohexanesulfamic acid in tetrahydrofuran to give 6.7 g pure product, m. 140°-1°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974157 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-423e237ddafd419685aa66d3d10b687c |
| Source note | uspto-grants-1976_08 |