Hydrochloric Acid → HCID 68138797, compound

Participants

Reaction Steps

The procedure of Example I(c) is followed using 6.5 ml acetyl chloride and 11.5 g 2-(3,4-Dimethoxyphenyl)-1-(2-dimethylamino-1-methylethyl)cyclohexanol and a reaction time of 6 hours to give 9.5 g. crude HCl salt which is dissolved in 50 ml isopropanol and diluted with 440 ml tetrahydrofuran and 60 ml ether to give 7.1 g product, m. 200°.

Provenance & Evidence