HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178421583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 178421584 | HCID 178421584 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178421583 | HCID 178421583 | — |
Reaction Steps
A stirred solution of (1-oxo-2-cyclopentyl-2-methyl-6,7-dichloro-5-indanyloxymethyl)tetrazole (5.7 g., 0.015 mole) and hydroxylamine hydrochloride (3.2 g., 0.045 mole) in pyridine (60 ml.) is heated at 95°C. on a steam bath for 30 hours then poured into aqueous hydrochloric acid affording 5-(1-hydroximino-2-cyclopentyl-2-methyl-6,7-dichloro-5-indanyloxymethyl)tetrazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974212 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-1d8b83055284418c85d493d9f5003ca0 |
| Source note | uspto-grants-1976_08 |