HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 53696864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 53961811 | HCID 53961811 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 53696864 | HCID 53696864 | — |
Reaction Steps
2-(4-Methoxycarbonylstyryl) pyridine (2.00g) and 20% w/v aqueous sodium hydroxide (100 ml) were stirred and refluxed for 2 hours. The reaction mixture was cooled, acidified with glacial acetic acid the solid filtered off, dried and recrystallised from ethanol. This gave 1.68 g (90%) 2 Carboxy styryl) pyridine MPT 228°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03974282 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-5663f30993fa45a8b8e15cd24c360db2 |
| Source note | uspto-grants-1976_08 |