HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6,6-Trimethyl-1-(1-hydroxy-3-butenyl)-1-cyclohexene → 2,6,6-Trimethyl-1-[3-methyl-3-butenoyl]-1-cyclohexene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6,6-Trimethyl-1-(1-hydroxy-3-butenyl)-1-cyclohexene | HCID 12420321 | — |
| Reactant | 2,6,6-Trimethyl-1-[1-hydroxy-3-methyl-3-butenyl]-1-cyclohexene | HCID 23338058 | — |
| Product | 2,6,6-Trimethyl-1-[3-methyl-3-butenoyl]-1-cyclohexene | HCID 23338084 | — |
Reaction Steps
By replacing hereabove 2,6,6-trimethyl-1-[1-hydroxy-3-butenyl]-1-cyclohexene with 2,6,6-trimethyl-1-[1-hydroxy-3-methyl-3-butenyl]-1-cyclohexene (nD20 = 1.4939; d420 = 0.9270), 2,6,6-trimethyl-1-[3-methyl-3-butenoyl]-1-cyclohexene was obtained; ndD20 = 1.4862; d420 = 0.9307.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975310 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-8124431facd84e38bd14608a1d4f2840 |
| Source note | uspto-grants-1976_08 |