1-Bromooctane → HCID 54426749, compound

Participants

Reaction Steps

A mixture of 56.4 parts of 2,2,6,6-tetramethylpiperidine and 38.6 parts of 1-bromooctane was heated at 125°-30°C for 120 hours. The cooled reaction mixture was filtered to remove 2,2,6,6-tetramethylpiperidine hydrobromide formed during the reaction. Fractional distillation of the residue gave 1-n-octyl-2,2,6,6-tetramethylpiperidine having a boiling point of 168°C/17 mm of Hg.

Provenance & Evidence