HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octanol → HCID 21245368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octanol | HCID 957 | — |
| Reactant | Lithium amide | HCID 24532 | — |
| Reactant | HCID 20238190 | HCID 20238190 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21245368 | HCID 21245368 | — |
Reaction Steps
A mixture of 45.4 parts of 1-ethoxycarbonylmethyl-2,2,6,6-tetramethylpiperidine, 36.5 parts of 1-octanol and 0.5 part of lithium amide was heated at 110°-115°C for 48 hours, the ethyl alcohol formed during the reaction being removed by distillation. Fractional distillation of the reaction mixture gave 1-octoxycarbonylmethyl-2,2,6,6-tetramethylpiperidine having a boiling point of 120°C/0.005 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975357 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-f68c3c4837f84f6da5dc0e3ceade9d7e |
| Source note | uspto-grants-1976_08 |