HRID1283401

反应详情

EQUATION

反应方程式

HRID 1283401 的结构方程式

PROCEDURE

实验过程

This was prepared in 95% yield by reaction of 3-(3-amino-4-methoxybenzoyl)-propionic acid with hydrazine hydrate in ethanolic solution at reflux temperature for 5 hours. It had m.p. 218°-220°C after crystallisation from ethanol.

WORKUP

后处理

  1. temperatureat reflux temperature for 5 hours
  2. customafter crystallisation from ethanol