HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Diethylethylenediamine → Tiapride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Diethylethylenediamine | HCID 60993 | — |
| Reactant | 5-Mesyl-o-anisic acid | HCID 170840 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Tiapride | HCID 5467 | — |
Reaction Steps
2.3 g (0.01 mol) of 2-methoxy 5-methylsulfonylbenzoic acid, 2.9 g (0.025 mol) of N,N-diethyl ethylenediamine and 40 ml of dioxan are placed in a 100 ml balloon flask provided with a stirrer and a condenser.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975434 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-73c09dc60c3840659889add78b7c97db |
| Source note | uspto-grants-1976_08 |