HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 131710433, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 4-Fluorobenzoyl chloride | HCID 67879 | — |
| Reactant | 1-[1-(Piperidin-1-yl)cyclohexyl]methanamine | HCID 398402 | — |
| Product | HCID 131710433 | HCID 131710433 | — |
Reaction Steps
A mixture of 1-(1-aminomethylcyclohexyl) piperidine (1.5 g.), 4-fluorobenzoyl chloride (2 ml) and pyridine (10 ml) was allowed to stand at room temperature for 1 hr. The crystalline material produced was filtered (2.35 g. 86.6%) and afforded pale lemon rosettes of 1-(4-fluorobenzamido-methylcyclohexyl)piperidine, hydrochloride m.p. 243°-5° (Decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975443 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-56fbb9716c8b4366a2084391f6ebe297 |
| Source note | uspto-grants-1976_08 |