HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 54479703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | 1-Propanol | HCID 1031 | — |
| Reactant | HCID 21518480 | HCID 21518480 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 54479703 | HCID 54479703 | 31% |
Reaction Steps
1-(1-Oxido-thiomorpholino)-3-piperazino-5-chloro-isoquinoline was prepared analogous to Example 12 from 1-thiomorpholino-3-piperazino-5-chloro-isoquinoline in dilute sulfuric acid by oxidation with hydrogen peroxide. M.p. 215°-217°C (from n-propanol); yield: 31% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975524 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-97f77a119f3640c3bbb8ffe52d19d014 |
| Source note | uspto-grants-1976_08 |