HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 86733847, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 21518487 | HCID 21518487 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 86733847 | HCID 86733847 | 31% |
Reaction Steps
1-(1-Oxido-thiomorpholino-3-piperazino-5-fluoro-isoquinoline was prepared analogous to Example 12 from 1-thiomorpholino-3-piperazino-5-fluoro-isoquinoline by oxidation with hydrogen peroxide in dilute sulfuric acid. M.p. 213°-215°C (from n-propanol/petroleum ether). Yield: 31% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975524 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-bb53838be7a54b37979d8c6ae41e755e |
| Source note | uspto-grants-1976_08 |