HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Peroxide → HCID 54292749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Maleate(2-) | HCID 5288227 | — |
| Reactant | HCID 21518484 | HCID 21518484 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 54292749 | HCID 54292749 | 41% |
Reaction Steps
1-(1-Oxido-thiomorpholino)-3-piperazino-5-nitro-isoquinoline was prepared analogous to Example 12 from 1-thiomorpholino-3-piperazino-5-nitro-isoquinoline hydrochloride by oxidation with hydrogen peroxide in dilute sulfuric acid. M.p. of its maleate: 231°-233°C (from isopropanol). Yield: 41% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975524 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-ef4ab6a10e6f4881826bf1ded8f03bc5 |
| Source note | uspto-grants-1976_08 |