HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Butylbenzofuran → 2-n-Butyl-3-(2'-methoxybenzoyl)benzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Butylbenzofuran | HCID 77951 | — |
| Reactant | 2-Methoxybenzoyl chloride | HCID 88969 | — |
| Product | 2-n-Butyl-3-(2'-methoxybenzoyl)benzofuran | HCID 21518595 | — |
Reaction Steps
Acylation of 9.4 g. (0.054 mol.) of 2-n-butylbenzofuran with 9.9 g. (0.058 mol.) of o-anisoyl chloride according to the procedure described in Example 10 gave 2-n-butyl-3-(2'-methoxybenzoyl)benzofuran which was demethylated with pyridine hydrochloride as previously described to give 2-n-butyl-3-(2'-hydroxybenzoyl)benzofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03975537 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-8015124e0b4a4cfd9a369adf01403c48 |
| Source note | uspto-grants-1976_08 |