HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrotoluene → HCID 12906240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrotoluene | HCID 6944 | — |
| Reactant | Dimethylformamide diethylacetal | HCID 70913 | — |
| Product | HCID 12906240 | HCID 12906240 | — |
Reaction Steps
A solution of 27.4 g. of o-nitrotoluene and 31.2 g. of 95% N,N-dimethylformamide diethyl acetal was heated under a nitrogen atmosphere in a 165° oil bath for 22 hours with continuous distillation of the ethanol formed in the reaction through a distillation head and descending condenser.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03976639 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-e86314bedd22474e870d687754ccbb5c |
| Source note | uspto-grants-1976_08 |