HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 2-Bromo-6-(trifluoromethyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2'-Bromo-6'-trifluoromethylacetanilide | HCID 23253853 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | 2-Bromo-6-(trifluoromethyl)aniline | HCID 94059 | — |
Reaction Steps
2'-Bromo-6'-trifluoromethylacetanilide in 50% aqueous sulfuric acid is warmed on a steam bath for 2 hours, then refluxed for 1 hour. Cooling and dilution with water gives 2-bromo-6-trifluoromethylaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03976633 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-30256f537cbf4c6fb992bba3912c1689 |
| Source note | uspto-grants-1976_08 |