HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 54325562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 54268713 | HCID 54268713 | — |
| Product | HCID 54325562 | HCID 54325562 | — |
Reaction Steps
The product of Example 17 is dissolved in trifluoroacetic acid and the solution is stored at room temperature for one hour. The mixture is then concentrated to dryness in vacuo, and the residue is acylated with t-butyloxycarbonyl azide by the procedure described in Example 13 to obtain 3-carboxy-1-[(t-butyloxy)carbonyl]-2-pyrrolidineheptanoic acid phenylmethyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03976660 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-972c3d0e568542539a7c58a900f6b4b9 |
| Source note | uspto-grants-1976_08 |