HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 885478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Chloro-4-hydroxy-5-methoxybenzaldehyde | HCID 29622 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 885478 | HCID 885478 | — |
Reaction Steps
5-Chlorovanillin (60 g., 0.32 m.), 46.8 g. of potassium carbonate (0.34 m.), 1.9 g. of sodium iodide in 1.4 l. of ethanol and 46.8 g. (0.37 m.) of benzyl chloride in 200 ml. of ethanol are reacted to give 4-benzyloxy-5-chloro-3-methoxybenzaldehyde as an orange liquid which is employed for conversion of the epoxide without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03976695 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-0f13a5119de54429be85b946d146f855 |
| Source note | uspto-grants-1976_08 |