HRID1284011
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
In a three-neck flask there are introduced successively 2.04 g of methyl isothiocyanate, 20 ml heptane and, over the course of 5 minutes, a solution of 7.1 g 4-cyclohexyl-1-morpholyl-cyclohex-1-ene in 80 ml heptane and the reaction mixture is kept under vigourous stirring for 18 hours at room temperature.
WORKUP
后处理
- customover the course of 5 minutes