Methyl isothiocyanate → 4-Cyclohexyl 2-methylthiocarbamoyl 1-morpholyl cyclohex-1 ene

Participants

Reaction Steps

In a three-neck flask there are introduced successively 2.04 g of methyl isothiocyanate, 20 ml heptane and, over the course of 5 minutes, a solution of 7.1 g 4-cyclohexyl-1-morpholyl-cyclohex-1-ene in 80 ml heptane and the reaction mixture is kept under vigourous stirring for 18 hours at room temperature.

Provenance & Evidence