HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylhydrazine → 5-Cyclohexyl 3-phenylamino 2-methyl 4,5,6,7-tetrahydroindazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylhydrazine | HCID 81921 | — |
| Reactant | (Prop-2-yn-1-yl)hydrazine | HCID 15567523 | — |
| Reactant | 4-Cyclohexyl 2-phenylthiocarbamoyl cyclohexanone | HCID 21515296 | — |
| Reactant | 5-Cyclohexyl 3-phenylamino 2-propynyl 4,5,6,7-tetrahydroindazole | HCID 86733876 | — |
| Reactant | 5-Cyclohexyl 3-phenylamino 2-propenyl 4,5,6,7-tetrahydro indazole | HCID 86733877 | — |
| Product | 5-Cyclohexyl 3-phenylamino 2-methyl 4,5,6,7-tetrahydroindazole | HCID 21515290 | — |
Reaction Steps
In a similar manner starting from 6.9 g of 4-cyclohexyl 2-phenylthiocarbamoyl cyclohexanone and from 1.68 g propargylhydrazine, 4.10 g of 5-cyclohexyl 3-phenylamino 2-propynyl 4,5,6,7-tetrahydroindazole are obtained. In a similar manner starting from 6.9 g 4-cyclohexyl 2-phenylthiocarbamoyl cyclohexanone and 1.70 g allylhydrazine, 5.4 g of 5-cyclohexyl 3-phenylamino 2-propenyl 4,5,6,7-tetrahydro indazole are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03978044 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-870667a1928e475c8401cd45bea106d0 |
| Source note | uspto-grants-1976_08 |