Pyrrolidine → HCID 13433237, compound

HRID 1284017Notes

Reaction equation

HRID 1284017 reaction equation
[C:1]1([C:7]2([C:14]#[N:15])[CH2:12][CH2:11][C:10](=O)[CH2:9][CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH:16]1[CH2:20][CH2:19][CH2:18][CH2:17]1>>[C:14]([C:7]1([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH2:12][CH2:11][C:10]([N:16]2[CH2:20][CH2:19][CH2:18][CH2:17]2)=[CH:9][CH2:8]1)#[N:15]

Participants

3

Reactant 2

HCID 31268PyrrolidineHCID 912824-Oxo-1-phenylcyclohexanenitrile

Product 1

HCID 13433237HCID 13433237, compound

Procedure

Using the procedure of step A at example 1 and starting from 79.6 g of 4-phenyl 4-cyanocyclohexanone and 56.8 g pyrrolidine there is obtained with a theoretical yield 4-cyano 4-phenyl 1-pyrrolidino cyclohex-1-ene.

Workup

  1. customthere is obtained with

Sources & evidence

ORD record
ord-2d680955dacc48d08def201205bd4138
Source dataset
uspto-grants-1976_08
Patent number
US03978044

Reaction notes

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