HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → 5-Hydrazino-1,3-dihydropyrrolo[4,3,2-de]isoquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 5-Ethoxy-1,3-dihydropyrrolo[4,3,2-de]isoquinoline | HCID 21515522 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5-Hydrazino-1,3-dihydropyrrolo[4,3,2-de]isoquinoline | HCID 3041087 | — |
Reaction Steps
Similarly, treatment of equimolar amounts of 5-ethoxy-1,3-dihydropyrrolo[4,3,2-de]isoquinoline hydrofluoroborate, described in Example 5, and hydrazine hydrate in methanol gives 5-hydrazino-1,3-dihydropyrrolo[4,3,2-de]isoquinoline hydrofluoroborate, mp 263° - 265°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03978066 |
| Source dataset | uspto-grants-1976_08 |
| ORD ID | ord-36039045e4a14bdcbc0f6ec466bb196b |
| Source note | uspto-grants-1976_08 |